HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyrohydrazide → HCID 86152458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyrohydrazide | HCID 77079 | — |
| Reactant | 1-(3-Chloropyridin-4-yl)ethan-1-one | HCID 12742467 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86152458 | HCID 86152458 | 25% |
Reaction Steps
A mixture of 5.20 gm (0.0335 mole) of 4-acetyl-3-chloropyridine, 3.43 gm (0.0336 mole) of butyric acid hydrazide and 100 ml of ethanol was refluxed 18 hr. The mixture was chilled in the freezer. The solid which separated was collected to give 2.01 gm (25%) of white solid having a melting point of 103.8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05023334 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-117de7e8f9e74e56a1aa4df5aa72cbf8 |
| Source note | uspto-grants-1991_06 |