HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl bromide → HCID 15926211, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | HCID 15926210 | HCID 15926210 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15926211 | HCID 15926211 | — |
Reaction Steps
The N-methyl 2-benzyl-4-chloroaniline (10.8 g) in solution in ethyl acetate is treated at 5° C. with 4.9 ml of bromoacetyl bromide. After 1 hour at room temperature, decantation and washing with water, the solution is concentrated. Upon crystallization, N-methyl 2'-benzyl-4'-chloro-bromoacetanilide is obtained (12.21 g). MP=78° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025015 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-d88c985b3e9648269ede4175f0f2c584 |
| Source note | uspto-grants-1991_06 |