Chlorosulfamic acid → HCID 19829505, compound

HRID 1493980Notes

Reaction equation

HRID 1493980 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][C:7]1[CH:8]=[C:9]([CH:14]=[CH:15][CH:16]=1)[O:10][CH2:11][CH2:12][OH:13]>>[CH3:6][C:7]1[CH:8]=[C:9]([CH:14]=[CH:15][CH:16]=1)[O:10][CH2:11][CH2:12][O:13][S:1](=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 83611Ethanol, 2-(3-methylphenoxy)-

Product 1

HCID 19829505HCID 19829505, compoundYield 47%

Procedure

The title compound was prepared by procedures of Example 4 from sulfamoyl chloride and 2-(3-methylphenoxy)ethanol in 47% yield [recrystallizing ethyl ether-petroleum ether (30°-60° C.)]. A white solid, mp 76°-78° C., was obtained.

Workup

  1. customA white solid, mp 76°-78° C., was obtained

Sources & evidence

ORD record
ord-eff5bf37f28c4b8fbc3d56cf286bf28b
Source dataset
uspto-grants-1991_06
Patent number
US05025031

Reaction notes

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