HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfamic acid → Sulfamic acid 2-(3-methylphenoxy)ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Reactant | Ethanol, 2-(3-methylphenoxy)- | HCID 83611 | — |
| Product | Sulfamic acid 2-(3-methylphenoxy)ethyl ester | HCID 19829505 | 47% |
Reaction Steps
The title compound was prepared by procedures of Example 4 from sulfamoyl chloride and 2-(3-methylphenoxy)ethanol in 47% yield [recrystallizing ethyl ether-petroleum ether (30°-60° C.)]. A white solid, mp 76°-78° C., was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025031 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-eff5bf37f28c4b8fbc3d56cf286bf28b |
| Source note | uspto-grants-1991_06 |