2-Phenoxy-1-propanol → 2-Phenoxypropanol sulfamate

Participants

Reaction Steps

The title compound was prepared by procedures of Example 16 from sulfamoyl chloride and 2-phenoxypropanol. The oil obtained was further purified by chromatography (silica gel, eluted with methylene chloride) and recrystallization to give the title compound as a colorless, viscous oil in 35% yield.

Provenance & Evidence