Chlorosulfamic acid → HCID 19108702, compound

HRID 1493989Notes

Reaction equation

HRID 1493989 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Cl:6][C:7]1[CH:8]=[C:9]([CH:14]=[CH:15][CH:16]=1)[O:10][CH2:11][CH2:12][OH:13]>>[Cl:6][C:7]1[CH:8]=[C:9]([CH:14]=[CH:15][CH:16]=1)[O:10][CH2:11][CH2:12][O:13][S:1](=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 802702-(3-Chlorophenoxy)ethanol

Product 1

HCID 19108702HCID 19108702, compoundYield 44%

Procedure

The title compound was prepared by procedures of Example 16 from sulfamoyl chloride and 2-(3-chlorophenoxy)ethanol. The oil obtained was further purified by column chromatography and recrystallization from ethyl ether-petroleum ether (30°-60° C.) to give a white solid, mp 66°-69° C., in 44% yield.

Workup

  1. customThe oil obtained
  2. customwas further purified by column chromatography and recrystallization from ethyl ether-petroleum ether (30°-60° C.)
  3. customto give a white solid, mp 66°-69° C.

Sources & evidence

ORD record
ord-05b88a9a0771459aa297dd4476cdd51b
Source dataset
uspto-grants-1991_06
Patent number
US05025031

Reaction notes

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