HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfamic acid → HCID 19108702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Reactant | 2-(3-Chlorophenoxy)ethanol | HCID 80270 | — |
| Product | HCID 19108702 | HCID 19108702 | 44% |
Reaction Steps
The title compound was prepared by procedures of Example 16 from sulfamoyl chloride and 2-(3-chlorophenoxy)ethanol. The oil obtained was further purified by column chromatography and recrystallization from ethyl ether-petroleum ether (30°-60° C.) to give a white solid, mp 66°-69° C., in 44% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025031 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-05b88a9a0771459aa297dd4476cdd51b |
| Source note | uspto-grants-1991_06 |