HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 11806775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 4-(Trifluoromethyl)phenol | HCID 67874 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 11806775 | HCID 11806775 | 78.7% |
Reaction Steps
This compound was prepared according to the procedure used in Example 56. A mixture of 9.6 g (0.059 mole) of α,α,α-trifluoro-p-cresol, 5.7 ml (9.2 g, 0.065 mole) of chlorosulfonyl isocyanate and 75 ml of toluene gave 11.2 g (70%) of white solid, mp 111°-112° C. (benzene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025031 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-9ed090c411ae480b80668444eb3faa97 |
| Source note | uspto-grants-1991_06 |