Methyl iodide → HCID 86744864, compound

Participants

Reaction Steps

The product of Example 116 (0.74 g, 1.5 mmol) was dissolved in 50 mL of acetone to which 2 mL of methyl iodide was added. A small amount (10 mL) of CH3NO3 was subsequently added to increase solubility. The reaction was allowed to proceed for 2 days, then the solid was collected to give 0.54 g (56% yield) of the title compound melting at 218°-221° C. and having the formula ##STR145## The structure of the product was confirmed by elemental analysis.

Provenance & Evidence