HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14986350, compound → Benzoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14986350 | HCID 14986350 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Benzoic Acid | HCID 243 | — |
Reaction Steps
A mixture of 0.6 g of 3-chloro-4-[6-[2,3-bis(phenylmethoxy)phenyl]hexyloxy]benzoic acid and 60 mg of 10% palladium on carbon in 20 ml of tetrahydrofuran was stirred in a hydrogen atmosphere for 6 hours. Workup as in Example 36 and recrystallization from ethyl acetate-hexane gave 0.24 g, mp benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025036 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-94ad0ae1535a4514b71b3d0352224edc |
| Source note | uspto-grants-1991_06 |