Acetic Acid → HCID 19827430, compound

Participants

Reaction Steps

0.0766 mol (20 g) of 3-nitro-4-(β-bromoethyl)-aminophenol is heated for 20 minutes, at 60° C., in 60 ml of a 40% strength aqueous solution of dimethylamine. The reaction medium is poured into 300 ml of iced water and then neutralised with acetic acid. The expected product precipitates. It is filtered off, washed with water and recrystallised from ethanol. After drying in vacuo, it melts at 151° C.

Provenance & Evidence