HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Chlorophenylacetic acid → Acetyl chloride, 2-(2-chlorophenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Chlorophenylacetic acid | HCID 17124 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Acetyl chloride, 2-(2-chlorophenyl)- | HCID 182669 | 99% |
Reaction Steps
A mixture of 30.0 g (0.176 mol) of o-chlorophenylacetic acid and 40 ml of thionyl chloride was stirred for 18 hours. The volatiles then were removed in vacuo to give 32.76 g (99.0%) of o-chlorophenylacetyl chloride as a transparent, pale yellow, mobile liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05026707 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-e4a7a57297514dbc8b2cf4d395ffda55 |
| Source note | uspto-grants-1991_06 |