HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Thioglycolate → HCID 19828252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Thioglycolate | HCID 16907 | — |
| Reactant | Lithium amide | HCID 24532 | — |
| Reactant | 1-Octyloxy-2,2,6,6-tetramethylpiperidin-4-ol | HCID 11346683 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19828252 | HCID 19828252 | — |
Reaction Steps
The general procedure of Example 1 is followed using 2.09 grams (7.0 mmol) of 1-octyloxy-4-hydroxy-2,2,6,6-tetramethylpiperidine, 0.74 gram (7.0 mmol) of methyl thioglycolate and 0.17 gram of lithium amide in 50 ml of toluene to afford the title compound after purification by silica gel chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05026750 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-171fc11990b641149d2146fa52b16df9 |
| Source note | uspto-grants-1991_06 |