HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-mercaptopropionate → HCID 23173708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-mercaptopropionate | HCID 18050 | — |
| Reactant | Lithium amide | HCID 24532 | — |
| Reactant | 1-Cyclohexyloxy-2,2,6,6-tetramethyl-piperidin-4-ol | HCID 11322811 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23173708 | HCID 23173708 | — |
Reaction Steps
The general procedure of Example 1 is followed using 2.00 grams (7.8 mmol) of 1-cyclohexyloxy-4-hydroxy-2,2,6,6-tetramethylpiperidine, 0.18 gram of lithium amide and 0.94 gram (7.8 mmol) of methyl 3-mercaptopropionate in 50 ml of toluene to afford the title compound after purification by silical gel chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05026750 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-e6d441c05e634b8ca3527c1b42154c26 |
| Source note | uspto-grants-1991_06 |