Sodium Hydroxide → HCID 19828691, compound

Participants

Reaction Steps

2,5-Dimercapto-1,3,4-thiadiazole(51.64 grams, 0.34 moles) and isopropanol(150 ml) were added to the reaction flask. Dodecyl glycidyl ether(87.35 grams, 0.34 moles) was slowly added with cooling to maintain the temperature below 25° C. Then sodium hydroxide(0.05 grams) was added followed by butyl glycidyl ether (44.91 grams, 0.34 moles). The reaction mixture was refluxed for 15 minutes and the solvent was stripped off by using a rotary evaporator. The product was characterized by infrared absorption bands at 3200, 2900, 1460, 1385, 1260, 1120, 1050, and 710 cm-1.

Provenance & Evidence