Phenyl glycidyl ether → HCID 15144527, compound

Participants

Reaction Steps

Phenyl glycidyl ether (179.4 grams, 1.20 moles) and isopropanol (200 ml) were charged into the reaction vessel. 2,5-Dimercapto-1,3,4-thiadiazole (85 grams, 0.568 moles) was added in increments and with stirring. The reaction mixture was refluxed for 5 minutes. The solvent was stripped off by using a rotary evaporator at about 20 mm Hg and 115° C. The product solidified on cooling and was characterized by the infrared absorption bands at 3400, 3060, 2920, 1600, 1500, 1380, 1240, 1040, 750, and 690 cm-1.

Provenance & Evidence