HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 19828704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 19828697 | HCID 19828697 | — |
| Catalyst | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | HCID 19828704 | HCID 19828704 | — |
Reaction Steps
2-Acetyl-2,3-dihydro-1H-indene-2-carbonitrile (32.9 g) was dissolved in diethyl ether (33 ml). Aluminium chloride (0.17 g) was added. Bromine (28.4 g) was added dropwise at room temperature and the disappearance of the bromine colour was observed. The ether solution was washed with a Na2CO3 -solution and with water, dried over MgSO4, and evaporated. 35.7 g of crude product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05026868 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-3efc1499b880408fa50348fc819f11be |
| Source note | uspto-grants-1991_06 |