HRID1494730

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC1COc2c(F)c(F)cc3c(=O)c(C(=O)O)cn1c23

HCID534278

未命名化合物

HCID14795861

2,3-Dihydro-1H-isoindol-4-amine

C8H10N2

PRODUCTS

生成物

结构：CC1COc2c(N3Cc4cccc(N)c4C3)c(F)cc3c(=O)c(C(=O)O)cn1c23

HCID15167914

未命名化合物

收率 53.9%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

157 mg of 9,10-difluoro-2,3-dihydro-3-methyl-7-oxo-7H-pyrido[1,2,3-de][1,4]-benzoxazine-6-carboxylic acid, 242 mg of 4-aminoisoindoline, and 1.5 ml of anhydrous DMF were processed in the same manner as in Example 2 to produce 119 mg of the target compound.