HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fluoren-9-ol → 5-[7-(9H-fluoren-9-yloxy)heptyl]-3-methyl-isoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fluoren-9-ol | HCID 74318 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 5-(7-Bromoheptyl)-3-methylisoxazole | HCID 13316967 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 5-[7-(9H-fluoren-9-yloxy)heptyl]-3-methyl-isoxazole | HCID 5272761 | — |
Reaction Steps
The sodium salt of 9-hydroxyfluorene was made by reacting sodium metal in anhydrous benzene before the etherization with 7-(3-methylisoxazol-5-yl)-heptyl bromide in the same solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05026848 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-8ef4b7c73bb247dbb519a70e9aaa115f |
| Source note | uspto-grants-1991_06 |