Lauryldimethylamine → Benzenemethanaminium, N-dodecyl-4-ethenyl-N,N-dimethyl-, chloride (1:1)

HRID 1496787Notes

Reaction equation

HRID 1496787 reaction equation
[CH:1]([C:3]1[CH:10]=[CH:9][C:6]([CH2:7][Cl:8])=[CH:5][CH:4]=1)=[CH2:2].[CH3:11][N:12]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH3:13]>>[Cl-:8].[CH3:11][N+:12]([CH3:13])([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH2:7][C:6]1[CH:9]=[CH:10][C:3]([CH:1]=[CH2:2])=[CH:4][CH:5]=1

Participants

3

Reactant 2

HCID 8168LauryldimethylamineHCID 74126p-Vinylbenzyl chloride

Product 1

HCID 6453318Benzenemethanaminium, N-dodecyl-4-ethenyl-N,N-dimethyl-, chloride (1:1)

Procedure

Into a 200 ml flask were added 29.8 g of 4-vinylbenzyl chloride and 50 g of N,N-dimethyldodecylamine. The reaction mixture was stirred at room temperature for 24 h. The solid precipitate from the reaction was filtered, washed with diethyl ether, and dried under vacuum at room temperature.

Workup

  1. filtrationThe solid precipitate from the reaction was filtered
  2. washwashed with diethyl ether
  3. customdried under vacuum at room temperature

Sources & evidence

ORD record
ord-fbe17be959cd45d1827981ec595a85f8
Source dataset
uspto-grants-2015_12
Patent number
US09199203B2

Reaction notes

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