Pentane → HCID 86643015, compound

HRID 1496788Notes

Reaction equation

HRID 1496788 reaction equation
[C:1]([F:5])([CH3:4])([CH3:3])[CH3:2].[CH3:6][CH2:7][CH2:8][CH2:9][CH3:10]>>[C:1]([F:5])([CH3:4])([CH3:3])[CH3:2].[CH3:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 8003Pentane2×HCID 9626Propane, 2-fluoro-2-methyl-2×

Product 1

HCID 86643015HCID 86643015, compound

Procedure

500 mL of cold n-pentane kept at 0° C. was poured in a glass graduated cylinder. To the n-pentane was added 2.3 mL of tert-butyl fluoride also kept at 0° C. The resulting solution was thoroughly mixed and analyzed by CAP-GC by the CGSB method for gasoline. The concentration of the tert-butyl fluoride was found to be 0.43 wt %. The solution was kept in the refrigerator at 0° C.

Workup

  1. customkept at 0° C.
  2. additionwas poured in a glass
  3. customalso kept at 0° C
  4. additionThe resulting solution was thoroughly mixed
  5. customwas kept in the refrigerator at 0° C.

Sources & evidence

ORD record
ord-75a1ccdbff3846bf99d445f7cb52e3b0
Source dataset
uspto-grants-2015_12
Patent number
US09199222B2

Reaction notes

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