Pentane → HCID 86643015, compound
Reaction equation
[C:1]([F:5])([CH3:4])([CH3:3])[CH3:2].[CH3:6][CH2:7][CH2:8][CH2:9][CH3:10]>>[C:1]([F:5])([CH3:4])([CH3:3])[CH3:2].[CH3:6][CH2:7][CH2:8][CH2:9][CH3:10]Participants
3
Procedure
Approximately 220 mL of cold n-pentane kept at 0° C. was poured in a glass graduated cylinder. To the n-pentane was added approximately 1.7 mL of tert-butyl fluoride which was also kept at 0° C. The solution was mixed thoroughly and analyzed by CAP-GC using the CGSB (Canadian General Standards Board, 3.0 14.3-99) method for gasoline. The concentration of tert-butyl fluoride was 0.615 vol %. The solution was kept in the refrigerator at 0° C. Lower concentrations of the tert-butyl fluoride-n-pentane stock solution was obtained by diluting with pentane. To obtain 0.45 vol % of tert-butyl fluoride, 60.5 mL of n-pentane was added to 159.5 mL of the stock solution.
Workup
- customkept at 0° C.
- additionwas poured in a glass
- customwas also kept at 0° C
- additionThe solution was mixed thoroughly
- customwas kept in the refrigerator at 0° C
Sources & evidence
- ORD record
- ord-0e7f31a3928f40df83a103718565aae1
- Source dataset
- uspto-grants-2015_12
- Patent number
- US09199222B2
Reaction notes
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