HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86712489, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86712490 | HCID 86712490 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86712489 | HCID 86712489 | — |
Reaction Steps
A 2 N aqueous solution of HCl was added in one portion to a solution of the bis-Boc derivative (8) synthesized above (1.658 g, 2.09 mmol) in THF (200 mL) and the mixture was stirred for 24 h at room temperature. The mixture was then evaporated to dryness under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199928B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-fecf971c3abc46e592faff2dc51b52c0 |
| Source note | uspto-grants-2015_12 |