HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 118105716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Acetylpiperazine | HCID 83795 | — |
| Reactant | 2-(Benzyloxy)-4-fluoro-1-nitrobenzene | HCID 11096908 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 118105716 | HCID 118105716 | — |
Reaction Steps
The compound obtained in Step 1 above (300 mg), N-acetylpiperazine (300 mg), and potassium carbonate (500 mg) were dissolved in dimethylformamide (3 mL) and reacted at 80° C. overnight. The dimethylformamide of the reaction mixture was removed under reduced pressure, and added with water to form a solid. The solid was filtered to obtain a target compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199944B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-2f9f3ef35785407ca688fb3ad245174a |
| Source note | uspto-grants-2015_12 |