Water → HCID 53269422, compound

Participants

Reaction Steps

4-chloro-2-fluoronitrobenzene (250 mg) and t-butylamine (0.40 mL) were dissolved in dimethyl sulfoxide (3.0 mL) and stirred at room temperature overnight. Then, the mixture was added with water and extracted with ethyl acetate. The thus obtained organic layer was washed with saturated brine, and the water was removed with sodium sulfate, and the solvent was removed by distillation under reduced pressure. The subsequent reaction was proceeded without further purification of the thus obtained compound.

Provenance & Evidence