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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1497048Generated: October 30, 2026

Nitrogen → HCID 86682927, compound

https://huagongshe.com/reaction/1497048

Reaction equation

Participants

RoleNameHCIDCharge
ReactantNitrogenHCID 947—
ReactantPyridineHCID 1049—
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 72947918HCID 72947918—
Solvent1,2-DimethoxyethaneHCID 8071—
ProductHCID 86682927HCID 86682927—

Reaction Steps

Acetic anhydride (288 μl, 3.0 mmol) was added to a stirred suspension of 6-chloro-4-phenylquinoline-2,3-dicarboxylic acid (100 mg, 0.31 mmol) in dimethoxyethane (1 ml) in an inert N2 atmosphere followed by the addition of pyridine (49 μl, 0.61 mmol) at room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09199938B2
Source datasetuspto-grants-2015_12
ORD IDord-dc9908b1c781484aacda83134385391d
Source noteuspto-grants-2015_12