HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitrogen → HCID 86682927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 72947918 | HCID 72947918 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 86682927 | HCID 86682927 | — |
Reaction Steps
Acetic anhydride (288 μl, 3.0 mmol) was added to a stirred suspension of 6-chloro-4-phenylquinoline-2,3-dicarboxylic acid (100 mg, 0.31 mmol) in dimethoxyethane (1 ml) in an inert N2 atmosphere followed by the addition of pyridine (49 μl, 0.61 mmol) at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-dc9908b1c781484aacda83134385391d |
| Source note | uspto-grants-2015_12 |