HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 71556488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 86682957 | HCID 86682957 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 71556488 | HCID 71556488 | — |
Reaction Steps
The title compound was prepared in analogy to example 20 step D from 6-chloro-4-phenyl-2-(2,2,2-trifluoro-ethyl)-quinoline-3-carboxylic acid methyl ester (60 mg, 0.16 mmol) and lithium iodide (212 mg, 1.58 mmol) in pyridine. Off white solid (9.5 mg, 16%). LC-MS: 364 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-1d1e295d09b248d8a36129868bbd8b8d |
| Source note | uspto-grants-2015_12 |