HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 71556489, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 86682958 | HCID 86682958 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 71556489 | HCID 71556489 | — |
Reaction Steps
The title compound was prepared in analogy to example 20 step D from 6-chloro-4-(3-chloro-4-fluoro-phenyl)-2-isopropyl-quinoline-3-carboxylic acid methyl ester (60 mg, 0.15 mmol) and lithium iodide in pyridine. Off white solid (43 mg, 74%). LC-MS: 376 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-33bb36213eaa4713abda3d5146b09a4c |
| Source note | uspto-grants-2015_12 |