HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → 6-Chloro-2-cyclopentyl-4-phenyl-quinoline-3-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 86682959 | HCID 86682959 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 6-Chloro-2-cyclopentyl-4-phenyl-quinoline-3-carboxylic acid | HCID 71556490 | — |
Reaction Steps
The title compound was prepared in analogy to example 20 step D from 6-chloro-2-cyclopentyl-4-phenyl-quinoline-3-carboxylic acid ethyl ester (35 mg, 0.09 mmol) and lithium iodide in pyridine. Off-white solid (15 mg, 46%). LC-MS: 350 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-41605986830d420f90f8e73b090324c7 |
| Source note | uspto-grants-2015_12 |