HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 71556492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 86682961 | HCID 86682961 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 71556492 | HCID 71556492 | — |
Reaction Steps
The title compound was prepared in analogy to example 20 step D from 6-chloro-2-(2-oxo-pyrrolidin-1-yl)-4-phenyl-quinoline-3-carboxylic acid ethyl ester (50 mg, 0.13 mmol) and LiI in pyridine. Yellow solid (11 mg, 24%). LC-MS: 367 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-89ea1e1d98cb42b29a7776d08c04bf87 |
| Source note | uspto-grants-2015_12 |