Ethyl isobutyrylacetate → HCID 86682962, compound

Participants

Reaction Steps

The title compound was prepared in analogy to example 10 step B from 4-chloro-2-(2-methoxy-phenylethynyl)-phenylamine (200 mg, 0.78 mmol) and 4-methyl-3-oxo-pentanoic acid ethyl ester (0.2 ml, 1.16 mmol) in anhydrous EtOH (8 ml). Light green liquid. (100 mg, 32% yield). LC-MS (ESI): 398 (M+H)+.

Provenance & Evidence