HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 71556551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 86682962 | HCID 86682962 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 71556551 | HCID 71556551 | — |
Reaction Steps
The title compound was prepared in analogy to example 20 step D from 6-chloro-2-isopropyl-4-(2-methoxy-benzyl)-quinoline-3-carboxylic acid ethyl ester (80 mg, 0.2 mmol) and lithium iodide (134.5 mg, 1.01 mmol) in pyridine. Off white solid (24 mg, 32%). LC-MS (ESI): 368 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-17ce773f22ea423fbb065a4958ed2725 |
| Source note | uspto-grants-2015_12 |