HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 71556621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 86682972 | HCID 86682972 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 71556621 | HCID 71556621 | — |
Reaction Steps
The title compound was prepared in analogy to example 20 step D from 6-chloro-2-diethylamino-4-phenyl-quinoline-3-carboxylic acid ethyl ester (50 mg, 0.13 mmol) and LiI in pyridine. Pale yellow solid (30 mg, 65%). LC-MS: 355 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-0467f4dcbc8743018f7cb4b3001d6671 |
| Source note | uspto-grants-2015_12 |