HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 71556622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 86682973 | HCID 86682973 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 71556622 | HCID 71556622 | — |
Reaction Steps
The title compound was prepared in analogy to example 20 step D from 6-chloro-4-phenyl-2-(2,2,2-trifluoro-1-methyl-ethoxy)-quinoline-3-carboxylic acid ethyl ester (100 mg, 0.26 mmol) and LiI in pyridine. Off white solid (55 mg, 53%). LC-MS: 396 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-31bda599fa574ab1a15752b6ce3eba30 |
| Source note | uspto-grants-2015_12 |