HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 86682981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 1-Chloro-2-ethynylbenzene | HCID 585995 | — |
| Reactant | 4-Chloro-2-fluoro-6-iodoaniline | HCID 2773650 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | HCID 86682981 | HCID 86682981 | — |
Reaction Steps
The title compound was prepared in analogy to example 10 step A from 4-chloro-2-fluoro-6-iodoaniline (500 mg, 1.84 mmol) and 1-chloro-2-ethynyl-benzene (302 mg, 2.21 mmol). Brown solid (1.05 g, 68%). Rf 0.3 (1:9 Ethyl acetate:heptane) as a bright blue spot under UV light.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-62f319d7c2a54ef0894cd890aa2a2782 |
| Source note | uspto-grants-2015_12 |