HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 71556818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 86682990 | HCID 86682990 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 71556818 | HCID 71556818 | — |
Reaction Steps
The title compound was prepared in analogy to example 20 step D from 6-chloro-4-(2-chloro-benzyl)-2-(2,2,2-trifluoro-ethyl)-quinoline-3-carboxylic acid ethyl ester (70 mg, 0.16 mmol) and LiI (212 mg, 1.58 mmol) in pyridine. Off white solid (15 mg, 23%). LC-MS: 412 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-19bcc7a14b19473188a9def3821bda69 |
| Source note | uspto-grants-2015_12 |