HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 71556887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86683011 | HCID 86683011 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 71556887 | HCID 71556887 | — |
Reaction Steps
The title compound was prepared in analogy to example 78 step E from 6-chloro-2-dimethylamino-4-(3-isopropyl-phenyl)-quinoline-3-carboxylic acid tert-butyl ester (75 mg, 0.18 mmol) and 4N HCl in dioxane. Off white solid (45 mg, 69%). LC-MS (ESI): 369 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-0bf42f88f76f44babf7497139a2e8876 |
| Source note | uspto-grants-2015_12 |