HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-ethynylbenzene → HCID 86683013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-ethynylbenzene | HCID 585995 | — |
| Reactant | HCID 67187010 | HCID 67187010 | — |
| Product | HCID 86683013 | HCID 86683013 | — |
Reaction Steps
The title compound was prepared in analogy to example 10 step A from 4-chloro-2-iodo-6-methoxy-phenylamine (300 mg, 1.06 mmol) and 1-chloro-2-ethynyl-benzene (174 mg, 1.27 mmol). Brown solid (220 mg, 71%). LC-MS (ESI): 292 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-e30b23f268a143eab8ea4116089e1cdb |
| Source note | uspto-grants-2015_12 |