HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isobutyrylacetate → HCID 86683014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isobutyrylacetate | HCID 81583 | — |
| Reactant | HCID 86683013 | HCID 86683013 | — |
| Product | HCID 86683014 | HCID 86683014 | — |
Reaction Steps
The title compound was prepared in analogy to example 10 step B from 4-chloro-2-(2-chloro-phenylethynyl)-6-methoxy-phenylamine (200 mg, 0.68 mmol) and 4-methyl-3-oxo-pentanoic acid ethyl ester (0.166 ml, 1.03 mmol). Brown solid (45 mg, 15%). LC-MS (ESI): 432 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199938B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-7f3c7d9df0f04e8f9c95ff554dc82645 |
| Source note | uspto-grants-2015_12 |