Diethylamine → HCID 86683065, compound

HRID 1497248Notes

Reaction equation

HRID 1497248 reaction equation
Cl[C:2]1[C:11]([C:12]2[NH:16][N:15]=[N:14][N:13]=2)=[C:10]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[C:9]2[C:4](=[CH:5][C:6]([F:24])=[C:7]([Cl:23])[CH:8]=2)[N:3]=1.[CH2:25]([NH:27][CH2:28][CH3:29])[CH3:26]>>[Cl:23][C:7]1[CH:8]=[C:9]2[C:4](=[CH:5][C:6]=1[F:24])[N:3]=[C:2]([N:27]([CH2:28][CH3:29])[CH2:25][CH3:26])[C:11]([C:12]1[N:13]=[N:14][NH:15][N:16]=1)=[C:10]2[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 8021DiethylamineHCID 178505399HCID 178505399, compound

Product 1

HCID 86683065HCID 86683065, compound

Procedure

The title compound was prepared in analogy to example 102 step C from 2,6-dichloro-7-fluoro-4-phenyl-3-(1H-tetrazol-5-yl)-quinoline (prepared as described in example 107 step B) and diethylamine. Light brown solid. MS (ESI): 397.4 (M+H)+.

Sources & evidence

ORD record
ord-98b3dbf6ce9c40549ef2b8946a38819f
Source dataset
uspto-grants-2015_12
Patent number
US09199938B2

Reaction notes

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