HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 90281947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 90281911 | HCID 90281911 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 90281947 | HCID 90281947 | — |
Reaction Steps
To benzyl N-(tert-butoxycarbonyl)-3-fluoro-L-phenylalaninate (659 mg) was added a 4 M solution of hydrogen chloride in dioxane (8.82 mL), followed by stirring at room temperature overnight. The reaction mixture was concentrated under reduced pressure to obtain benzyl 3-fluoro-L-phenylalaninate hydrochloride (505 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199927B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-25b714061e1343d5aef03ffaf1d4e3e6 |
| Source note | uspto-grants-2015_12 |