HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetamide → HCID 178474872, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetamide | HCID 178 | — |
| Reactant | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| Product | HCID 178474872 | HCID 178474872 | — |
Reaction Steps
A slurry of acetamide (500 mg, 8.46 mmol, 1 eq.) was heated neat in 1,1-dimethoxy-N,N-dimethylethanamine (5 mL) for 16 hours. The 1,1-dimethoxy-N,N-dimethylethanamine was removed by roto-evaporation to afford (Z)-N-(1-(dimethylamino)ethylidene)acetamide (2-1) as a dark yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09200001B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-a53ba4e38219409c8e37c63891a176ce |
| Source note | uspto-grants-2015_12 |