HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isovanillin → HCID 77531995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | HCID 68642532 | HCID 68642532 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 77531995 | HCID 77531995 | 86% |
Reaction Steps
In ethanol (5 ml), 2-(2,4-dichlorophenyl)-4-methylthiazole-5-carboxylic acid hydrazide (34 mg) and 3-hydroxy-4-methoxybenzaldehyde (19 mg) was heated under reflux for 25 hours. After the mixture was allowed to cool, the precipitated crystal was separated by filtration to give the title compound (42 mg, 86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09200008B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-8b4bad75250e4c7491903914deabd295 |
| Source note | uspto-grants-2015_12 |