HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → Oleyl methane sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | Oleyl Alcohol | HCID 5284499 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Oleyl methane sulfonate | HCID 6016198 | 96.4% |
Reaction Steps
Preparation A was repeated using 410 g oleyl alcohol, 2 liters DCM, 322 ml triethylamine, 194 g methane sulphonylchloride to yield 510 g (96%) oleyl methanesulphonate product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09200229B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-907c8480eb2f41e5826a86c35aba8efe |
| Source note | uspto-grants-2015_12 |