Iodoethane → 1-(5-Chloro-2-ethoxy-4-fluoro-3-iodophenyl)ethanone

HRID 1499800Notes

Reaction equation

HRID 1499800 reaction equation
[Cl:1][C:2]1[C:3]([F:13])=[C:4]([I:12])[C:5]([OH:11])=[C:6]([C:8](=[O:10])[CH3:9])[CH:7]=1.I[CH2:15][CH3:16]>>[Cl:1][C:2]1[C:3]([F:13])=[C:4]([I:12])[C:5]([O:11][CH2:15][CH3:16])=[C:6]([C:8](=[O:10])[CH3:9])[CH:7]=1

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 866668571-(5-Chloro-4-fluoro-2-hydroxy-3-iodophenyl)ethanone

Product 1

HCID 866669601-(5-Chloro-2-ethoxy-4-fluoro-3-iodophenyl)ethanone

Procedure

This compound was prepared according to the procedure of Example 13 Step 3, using 1-(5-chloro-4-fluoro-2-hydroxy-3-iodophenyl)ethanone and iodoethane as the starting materials. LCMS calculated for C10H10ClFIO2 (M+H)+: m/z=342.9; Found: 342.9.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-487006df1a7e407e9819c16a02fb2176
Source dataset
uspto-grants-2015_12
Patent number
US09199982B2

Reaction notes

Loading…