HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 4-iodopiperidine-1-carboxylate → tert-Butyl 4-(3-acetyl-5-chloro-2-methoxy-6-methylphenyl)piperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 4-iodopiperidine-1-carboxylate | HCID 10892302 | — |
| Reactant | 1-(5-Chloro-3-iodo-2-methoxy-4-methylphenyl)ethanone | HCID 86666797 | — |
| Product | tert-Butyl 4-(3-acetyl-5-chloro-2-methoxy-6-methylphenyl)piperidine-1-carboxylate | HCID 86677742 | — |
Reaction Steps
This compound was prepared using procedures analogous to those for Example 139 step 2 with 1-(5-chloro-3-iodo-2-methoxy-4-methylphenyl)ethanone and tert-butyl 4-iodopiperidine-1-carboxylate as starting materials. LCMS calculated for C20H28ClNO4Na (M+Na)+: m/z=404.1; Found: 404.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199982B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-a9c548494ae74334abcce583fd8cbb70 |
| Source note | uspto-grants-2015_12 |