HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → 3-[3-Chloro-5-(1-hydroxyethyl)-6-methoxy-2-methylphenyl]cyclobutanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 3-(3-Acetyl-5-chloro-2-methoxy-6-methylphenyl)cyclobutanone | HCID 86677750 | — |
| Product | 3-[3-Chloro-5-(1-hydroxyethyl)-6-methoxy-2-methylphenyl]cyclobutanol | HCID 86677752 | — |
Reaction Steps
This compound was prepared according to the procedure of Example 13 step 5, using of 3-(3-acetyl-5-chloro-2-methoxy-6-methylphenyl)cyclobutanone and sodium tetrahydroborate as the starting materials. LCMS calculated for C14H19ClO3Na (M+Na)+: m/z=293.1; Found: 293.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199982B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-71d09b652be143de9ab2fdb9cf209c4f |
| Source note | uspto-grants-2015_12 |