Butanal → HCID 86714715, compound

Participants

Reaction Conditions

Reaction Steps

Potassium carbonate (4.8 g, 35 mmol) was added to diisobutylamine (17.5 mL, 0.10 mol) under a nitrogen atmosphere, and the mixture was then cooled to −7° C. Butanal (9.0 mL, 0.10 mol) was added dropwise thereto over 10 minutes. The reaction mixture was gradually heated to room temperature and stirred for 19 hours. Insoluble matter was filtered off, and the filtrate was then concentrated under reduced pressure to obtain the title compound (13.6 g, yield: 74%) as a colorless oil substance.

Provenance & Evidence