Acetonitrile → HCID 86714716, compound

Participants

Reaction Conditions

Reaction Steps

Allyl bromide (1.30 mL, 15 mmol) was added to a mixture of (E)-but-1-enyldiisobutylamine (1.83 g, 10 mmol) and acetonitrile (5.5 mL) at room temperature under a nitrogen atmosphere, and the mixture was then stirred at an external temperature of 60° C. for 15 hours. The reaction mixture was cooled to room temperature and then concentrated under reduced pressure to obtain the title compound (2.79 g, 92%) as a red purple solid.

Provenance & Evidence