HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 58500175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Isobutyraldehyde | HCID 6561 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | 2-(2-Nitrovinyl)naphthalene | HCID 5357963 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 58500175 | HCID 58500175 | — |
Reaction Steps
The title compound was prepared from (E)-2-(2-nitrovinyl)naphthalene and isobutyraldehyde according to General Procedure. The enantiomeric excess was determined by HPLC with Chiralpak AS-H column at 210 nm (2-propanol:hexane=10:90), 1 mL/min, tmajor=16.2 min, tminor=18.0 min, [α]D20=+1.7 (c=1.8, CHCl3)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206090B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-db8e038d021249698c494c34747938b6 |
| Source note | uspto-grants-2015_12 |